AggieCHEN04
Chemical
- Feb 4, 2005
- 56
I work for an engeneering and construction company that has recently refurbished and is currently restarting an old Sulfinol plant. The plant was originally designed for processing 6 MMSCFD of high H2S gas with a 28 tray, 42" ID Contactor at 200 psig. Upon restarting it, we anticipate 2 MMSCFD of gas and have modified the contactor's treys to operate at 1/3 capacity.
The modifications include replacing the tray decks and adding channel baffles that effectively reduce the active area to a 16.5" wide by 20.75" long square. The new trays were designed for 110 gpm of solvent and 2 MMSCFD of gas but can operate at liquid rates as high as 250 gpm without creating liquid flooding or exceeding the maximum recommended downcomer velocity.
About 2 weeks ago we began circulating water through the system. We circulated water for approximately 2 days without incident. We then circulated the solvent, Sulfinol, without incident for a day or two until we noticed the tower swaying (by approximately 1 ft to 2 ft at the top) along the same direction as the liquid inlet nozzle and shut the system down. At this point we have not started flowing gas through the contactor.
Due to a lack of a minimum flow bypass we were pumping liquids in excess of 350 gpm initially but have recently added a bypass through the filter to maintain a flow rate of less than 200 gpm through the tower. Reducing the flow rate has not prevented the tower from swaying. We have tried heating the solvent and going back to circulating water but have not had success. We are currently installing an additional flow controlled bypass around the contactor to allow for as much as 100% turndown. After notifying the tray manufacturer of this problem, they confirmed that the trays and tower hydraulics should be able to handle up to 250 gpm of solvent. The tower has a 4" liquid inlet nozzle, which is considered to be on the small side for the 250 gpm, but the tower had originally operated at 275 gpm, fully loaded without swaying. We have performed an inspection of the tower and trays and have found no damage.
Please let us know if you have any insight into the root cause of this problem.
The modifications include replacing the tray decks and adding channel baffles that effectively reduce the active area to a 16.5" wide by 20.75" long square. The new trays were designed for 110 gpm of solvent and 2 MMSCFD of gas but can operate at liquid rates as high as 250 gpm without creating liquid flooding or exceeding the maximum recommended downcomer velocity.
About 2 weeks ago we began circulating water through the system. We circulated water for approximately 2 days without incident. We then circulated the solvent, Sulfinol, without incident for a day or two until we noticed the tower swaying (by approximately 1 ft to 2 ft at the top) along the same direction as the liquid inlet nozzle and shut the system down. At this point we have not started flowing gas through the contactor.
Due to a lack of a minimum flow bypass we were pumping liquids in excess of 350 gpm initially but have recently added a bypass through the filter to maintain a flow rate of less than 200 gpm through the tower. Reducing the flow rate has not prevented the tower from swaying. We have tried heating the solvent and going back to circulating water but have not had success. We are currently installing an additional flow controlled bypass around the contactor to allow for as much as 100% turndown. After notifying the tray manufacturer of this problem, they confirmed that the trays and tower hydraulics should be able to handle up to 250 gpm of solvent. The tower has a 4" liquid inlet nozzle, which is considered to be on the small side for the 250 gpm, but the tower had originally operated at 275 gpm, fully loaded without swaying. We have performed an inspection of the tower and trays and have found no damage.
Please let us know if you have any insight into the root cause of this problem.