Alfamath
Chemical
- Feb 1, 2007
- 1
The vacuum tower in Synthol Fractionation is giving us problems. The Vacuum Unit has low Cutpoint. I have read a lot of articles on vacuum revamp and considered so many things that can lead to such a problems. Here are the things that I have considered:
o Liquid misdistribution
o Internals Damage (those above the flash zone) due to high liquid levels
o Leakage of VGO from draw-off trays.
Is there a way of determining the above without shutting-down the Unit?
The Operation involved is dry (The bottoms is quenched by recycling cold VTB)
Operating Conditions of the Tower:
FZ Temperature = 285 0 C
FZ Pressure = 18 kPa
Pressure at Top = 11.46 kPa
Inlet Temperature = 290 - 295 0 C
% Recovered at 362 0 C is between 10 and 24 when the VTB is vacuum distilled in the lab.
Design Conditions of the Tower:
FZ Temperature = 291 0 C
FZ Pressure = 49 kPa
Pressure at Top = 48 kPa
Inlet Temperature = 293 0 C
Cutpoint = 370 – 420 0 C
There are two wash beds, one for hot slop wax reflux and another for hot HVGO reflux.
The Unit does not have a pre-condenser. It uses a Single stage twin ejector system to pull the vacuum. The tower has four packings; grid and pall rings are as wash beds and the other two for pumparound duties.
Four years ago, the vacuum tower was operating properly under similar operating conditions as the current one.
How does viscosity and density impact the fractionation in the Vacuum tower?
What can cause the lighter fractions to go in VTB?
I appreciate all the assistance I can have….
o Liquid misdistribution
o Internals Damage (those above the flash zone) due to high liquid levels
o Leakage of VGO from draw-off trays.
Is there a way of determining the above without shutting-down the Unit?
The Operation involved is dry (The bottoms is quenched by recycling cold VTB)
Operating Conditions of the Tower:
FZ Temperature = 285 0 C
FZ Pressure = 18 kPa
Pressure at Top = 11.46 kPa
Inlet Temperature = 290 - 295 0 C
% Recovered at 362 0 C is between 10 and 24 when the VTB is vacuum distilled in the lab.
Design Conditions of the Tower:
FZ Temperature = 291 0 C
FZ Pressure = 49 kPa
Pressure at Top = 48 kPa
Inlet Temperature = 293 0 C
Cutpoint = 370 – 420 0 C
There are two wash beds, one for hot slop wax reflux and another for hot HVGO reflux.
The Unit does not have a pre-condenser. It uses a Single stage twin ejector system to pull the vacuum. The tower has four packings; grid and pall rings are as wash beds and the other two for pumparound duties.
Four years ago, the vacuum tower was operating properly under similar operating conditions as the current one.
How does viscosity and density impact the fractionation in the Vacuum tower?
What can cause the lighter fractions to go in VTB?
I appreciate all the assistance I can have….