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Nitrogen Purity - Is 98 % too low?

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cougarfan

Mechanical
Nov 29, 2001
85
We are a batch chemical facility and purge and blanket with nitrogen. The nitrogen is generated with a nitorgen generator putting out a 99.5% purity with liquid nitrogen backup. Has anyone out there ventured to use a lower purity -say 98 % nitrogen.. We have a couple of proudcts that chemically will degrade so we will bring pure nitrogen to these tanks but we are looking at the safety aspects and it scares a lot of people to lower the purity.
 
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Infact 99.5% is low purity. I have seen applications (for PET) where the purity is maintained at 99.999% (actually it is 10ppm oxygen) As a pharma company we use 99.995% purity.

What is your concern? Do you want to increase the capacity of plant by reducing purity?

Generally there should not be any problem upto 7.5% oxygen (as far as ignition problems are concerned) But for oxidation, well it is your judgement.

Is it a PSA Nitrogen Generator?


 
There are chemical plants, for example, dealing with reactive aldehydes, that ask for inert gas having less than 80 ppm oxygen.
 
In general, 99.5% is commonly used in industry and is considered low in purity. Our O2 content is 10 ppm or lower.
It depends on your application.
 
As previously stated, oxygen concentration depends on the purpose of the blanket. For chemicals that are flammable/explosive, it would be best to contact NFPA or other agency for data on MOC (minimum oxygen for combustion) and ensure that your N2 has no more than ½ of that value. If your facility has hydrogen and is trying to inert vessels, then the 98% N2 would be a very bad choice.

If your N2 is coming off a PSA, then check flow very carefully. My experience with PSA (pressure swing absorption) units is that the rating of 98% N2 will be at a specific flowrate. As the flow goes up, the purity goes down.
 
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